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Lead perchlorate trihydrate is produced by the reaction of lead(II) oxide, lead carbonate, or lead nitrate by perchloric acid: . Pb(NO 3) 2 + HClO 4 → Pb(ClO 4) 2 + HNO 3. The excess perchloric acid was removed by first heating the solution to 125 °C, then heating it under moist air at 160 °C to remove the perchloric acid by converting the acid to the dihydrate.
The following chart shows the solubility of various ionic compounds in water at 1 atm pressure and room temperature (approx. 25 °C, 298.15 K). "Soluble" means the ionic compound doesn't precipitate, while "slightly soluble" and "insoluble" mean that a solid will precipitate; "slightly soluble" compounds like calcium sulfate may require heat to precipitate.
Glauber's salt – sodium sulfate.Na 2 SO 4; Sal alembroth – salt composed of chlorides of ammonium and mercury.; Sal ammoniac – ammonium chloride.; Sal petrae (Med. Latin: "stone salt")/salt of petra/saltpetre/nitrate of potash – potassium nitrate, KNO 3, typically mined from covered dungheaps.
Lead(II) sulfate is poorly soluble, as can be seen in the following diagram showing addition of SO 2− 4 to a solution containing 0.1 M of Pb 2+. The pH of the solution is 4.5, as above that, Pb 2+ concentration can never reach 0.1 M due to the formation of Pb(OH) 2. Observe that Pb 2+ solubility drops 10,000 fold as SO 2− 4 reaches 0.1 M.
A basic chloride of lead, PbCl 2 ·Pb(OH) 2, is known as Pattinson's white lead and is used as pigment in white paint. [17] Lead paint is now banned as a health hazard in many countries by the White Lead (Painting) Convention, 1921. PbCl 2 is an intermediate in refining bismuth (Bi) ore.
Lead(II) azide is prepared by the reaction of sodium azide and lead(II) nitrate in aqueous solution. [6] [5] Lead(II) acetate can also be used.[7] [8]Thickeners such as dextrin or polyvinyl alcohol are often added to the solution to stabilize the precipitated product.
It is then converted to the ammonium salt (NH 4) 2 PbCl 6 by adding ammonium chloride (NH 4 Cl). Finally, the solution is treated with concentrated sulfuric acid H 2 SO 4, to separate out lead tetrachloride. This series of reactions is conducted at 0 °C. The following equations illustrate the reaction: PbCl 2 + 2HCl + Cl 2 → H 2 PbCl 6
Lead(II) fluoride – PbF 2; Lead(II) hydroxide – Pb(OH) 2; Lead(II) iodide – PbI 2; Lead(II) nitrate – Pb(NO 3) 2; Lead(II) oxide – PbO; Lead(II) phosphate – Pb 3 (PO 4) 2; Lead(II) sulfate – Pb(SO 4) Lead(II) selenide – PbSe; Lead(II) sulfide – PbS; Lead(II) telluride – PbTe; Lead(II) thiocyanate – Pb(CNS) 2; Lead(II,IV ...