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Lead perchlorate trihydrate is produced by the reaction of lead(II) oxide, lead carbonate, or lead nitrate by perchloric acid: . Pb(NO 3) 2 + HClO 4 → Pb(ClO 4) 2 + HNO 3. The excess perchloric acid was removed by first heating the solution to 125 °C, then heating it under moist air at 160 °C to remove the perchloric acid by converting the acid to the dihydrate.
The following chart shows the solubility of various ionic compounds in water at 1 atm pressure and room temperature (approx. 25 °C, 298.15 K). "Soluble" means the ionic compound doesn't precipitate, while "slightly soluble" and "insoluble" mean that a solid will precipitate; "slightly soluble" compounds like calcium sulfate may require heat to precipitate.
Finally, the solution is treated with concentrated sulfuric acid H 2 SO 4, to separate out lead tetrachloride. This series of reactions is conducted at 0 °C. The following equations illustrate the reaction: PbCl 2 + 2HCl + Cl 2 → H 2 PbCl 6 H 2 PbCl 6 + 2 NH 4 Cl → (NH 4) 2 PbCl 6 + 2HCl (NH 4) 2 PbCl 6 + H 2 SO 4 → PbCl 4 + 2HCl + (NH 4 ...
Substance Formula 0 °C 10 °C 20 °C 30 °C 40 °C 50 °C 60 °C 70 °C 80 °C 90 °C 100 °C Barium acetate: Ba(C 2 H 3 O 2) 2: 58.8: 62: 72: 75: 78.5: 77: 75
Lead(II) sulfate is poorly soluble, as can be seen in the following diagram showing addition of SO 2− 4 to a solution containing 0.1 M of Pb 2+. The pH of the solution is 4.5, as above that, Pb 2+ concentration can never reach 0.1 M due to the formation of Pb(OH) 2. Observe that Pb 2+ solubility drops 10,000 fold as SO 2− 4 reaches 0.1 M.
Pb(NO 3) 2 + 2 HCl → PbCl 2 (s) + 2 HNO 3. It also forms by treatment of basic lead(II) compounds such as Lead(II) oxide and lead(II) carbonate. Lead dioxide is reduced by chloride as follows: PbO 2 + 4 HCl → PbCl 2 (s) + Cl 2 + 2 H 2 O. It also formed by the oxidation of lead metal by copper(II) chloride: Pb + CuCl 2 → PbCl 2 + Cu
K 2 CO 3; Pearlash – formed by baking potash in a kiln. Milk of sulfur (lac sulphuris) – formed by adding an acid to thion hudor (lime sulfur). Natron/soda ash/soda – sodium carbonate. Na 2 CO 3; Nitrum flammans – ammonium nitrate. Sugar of lead – lead(II) acetate, formed by dissolving lead oxide in vinegar.
Plumbide [Pb 5] 2−. Plumbide is an anion of lead atoms. There are three plumbide anions, written as Pb −, Pb 2− and Pb 4− with 3 oxidation states, -1, -2 and -4, respectively. A plumbide can refer to one of two things: an intermetallic compound that contains lead, or a Zintl phase compound with lead as the anion.