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Differential scanning calorimetry (DSC) is a thermoanalytical technique in which the difference in the amount of heat required to increase the temperature of a sample and reference is measured as a function of temperature. [1] Both the sample and reference are maintained at nearly the same temperature throughout the experiment.
Circular dichroism and differential scanning calorimetry both consume large amounts of protein and are low-throughput methods. The Thermofluor assay was the first high-throughput thermal shift assay and its utility and limitations has spurred the invention of a plethora of alternate methods.
Differential scanning calorimetry is a workhorse technique in many fields, particularly in polymer characterization. A modulated temperature differential scanning calorimeter (MTDSC) is a type of DSC in which a small oscillation is imposed upon the otherwise linear heating rate. This has a number of advantages.
An example is oxidation induction time by differential scanning calorimetry which can determine the amount of oxidation stabiliser present in a thermoplastic (usually a polyolefin) polymer material. Compositional analysis is often made using thermogravimetric analysis, which can separate fillers, polymer resin and other additives.
Modulated force TM (mf-TM) is when the force is changed with a frequency and amplitude; previously called DMA. The term modulated is a special variant of dynamic, used to be consistent with modulated temperature differential scanning calorimetry (mt-DSC) and other situations when a variable is imposed in a cyclic manner. [2]
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Differential thermal analysis (DTA) is a thermoanalytic technique that is similar to differential scanning calorimetry.In DTA, the material under study and an inert reference are made to undergo identical thermal cycles, (i.e., same cooling or heating programme) while recording any temperature difference between sample and reference. [1]
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