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An example of back titration, the Volhard method, named after Jacob Volhard, involves the addition of excess silver nitrate to the analyte; the silver chloride is filtered, and the remaining silver nitrate is titrated against ammonium thiocyanate, [1] with ferric ammonium sulfate as an indicator which forms blood-red [Fe(OH 2) 5 (SCN)] 2+ at the end point:
Back titration is a titration done in reverse; instead of titrating the original sample, a known excess of standard reagent is added to the solution, and the excess is titrated. A back titration is useful if the endpoint of the reverse titration is easier to identify than the endpoint of the normal titration, as with precipitation reactions
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A blank value in analytical chemistry is a measurement of a blank. The reading does not originate from a sample, but the matrix effects , reagents and other residues . These contribute to the sample value in the analytical measurement and therefore have to be subtracted.
Note that iodometry involves indirect titration of iodine liberated by reaction with the analyte, whereas iodimetry involves direct titration using iodine as the titrant. Redox titration using sodium thiosulphate, Na 2 S 2 O 3 (usually) as a reducing agent is known as iodometric titration since it is used specifically to titrate iodine. The ...
Advantages of Coulometric Titration Coulometric titration has the advantage that constant current sources for the generation of titrants are relatively easy to make. The electrochemical generation of a titrant is much more sensitive and can be much more accurately controlled than the mechanical addition of titrant using a burette drive.