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A vacuum tight seal and stability of the Büchner flask and filter are essential during the filtration process. A Büchner ring can be used with Büchner funnels, flasks, glass crucibles and Gooch crucibles. The wide flange and large surface contact ensures an excellent vacuum tight seal whilst the rings are easy to remove and offer excellent ...
Filtration is a unit operation that is commonly used both in laboratory and production conditions. This apparatus, adapted for laboratory work, is often used to isolate the product of synthesis of a reaction when the product is a solid in suspension. The product of synthesis is then recovered faster, and the solid is drier than in the case of a ...
Vacuum pumps are combined with chambers and operational procedures into a wide variety of vacuum systems. Sometimes more than one pump will be used (in series or in parallel) in a single application. A partial vacuum, or rough vacuum, can be created using a positive displacement pump that transports a gas load from an inlet port to an outlet ...
A partial vacuum is typically provided to the container below the filter media when laboratory filtration is challenging to speed up the filtering process. Depending on the type of filter being used, the majority of industrial filtration operations employ pressure or vacuum to speed up filtering and reduce the amount of equipment needed.
During filtration, the filtrate enters and is held by the flask while the residue remains on the filter paper in the funnel. The Büchner flask can also be used as a vacuum trap in a vacuum line to ensure that no fluids are carried over from the aspirator or vacuum pump (or other vacuum source) to the evacuated apparatus or vice versa.
Classically, filtration is tackled with a Schlenk filter, which consists of a sintered glass funnel fitted with joints and stopcocks. By fitting the pre-dried funnel and receiving flask to the reaction flask against a flow of nitrogen, carefully inverting the set-up and turning on the vacuum appropriately, the filtration may be accomplished ...