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Laboratory reflux apparatus for heating a chemical reaction Laboratory reflux apparatus. A mixture of reactants and solvent is placed in a suitable vessel, such as a round bottom flask. This vessel is connected to a water-cooled condenser, which is typically open to the atmosphere at the top.
In chemistry, a condenser is laboratory apparatus used to condense vapors – that is, turn them into liquids – by cooling them down. [1] Condensers are routinely used in laboratory operations such as distillation, reflux, and extraction. In distillation, a mixture is heated until the more volatile components boil off, the vapors are ...
Round-bottom flasks are often used to contain chemical reactions run by chemists, especially for reflux set-ups and laboratory-scale synthesis. [3] Boiling chips are added in distilling flasks for distillations or boiling chemical reactions to allow a nucleation site for gradual boiling. This nucleation avoids a sudden boiling surge where the ...
The Marcusson apparatus, Dean-Stark apparatus, Dean–Stark receiver, distilling trap, or Dean–Stark Head is a piece of laboratory glassware used in synthetic chemistry to collect water [1] [2] (or occasionally other liquid) from a reactor. It is used in combination with a reflux condenser and a distillation flask for the separation of water ...
The Liebig condenser (/ ˈ l iː b ɪ ɡ /, LEE-big) [1] or straight condenser is a piece of laboratory equipment, specifically a condenser consisting of a straight glass tube surrounded by a water jacket. In typical laboratory operation, such as distillation, the condenser is clamped to a retort stand in vertical or oblique
A Soxhlet extractor is a piece of laboratory apparatus [1] invented in 1879 by Franz von Soxhlet. [2] It was originally designed for the extraction of a lipid from a solid material. Typically, Soxhlet extraction is used when the desired compound has a limited solubility in a solvent, and the impurity is insoluble in that solvent. It allows for ...
Laboratory flasks are vessels or containers that fall into the category of laboratory equipment known ... to the rest of the apparatus (such as a reflux condenser or ...
The earliest laboratory condenser, a "Gegenstromkühler" (counter-flow condenser), was invented in 1771 by the Swedish-German chemist Christian Weigel. [2]By the mid-19th century, German chemist Justus von Liebig would provide his own improvements on the preceding designs of Weigel and Johann Friedrich August Göttling, with the device becoming known as the Liebig condenser.