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ACE mixture was most commonly made up in the ratio: 1 part alcohol, 2 parts chloroform, and 3 parts ether [2] although other ratios existed. See ' other preparations ' below. Chloroform (which was first used in 1847) used on its own produces myocardial depression, however the excitatory properties of the alcohol and ether contained with the ...
This page contains tables of azeotrope data for various binary and ternary mixtures of solvents. The data include the composition of a mixture by weight (in binary azeotropes, when only one fraction is given, it is the fraction of the second component), the boiling point (b.p.) of a component, the boiling point of a mixture, and the specific gravity of the mixture.
K b & K f [1] Chloroform: 1.48 61.2 3.88 –63.5 –4.90 K b & K f [1] Cyclohexane: 80.74 2.79 6.55 –20.2 Diethyl ether: 0.713 34.5 2.16 –116.3 –1.79 K b & K f [1] Methanol [4] 0.79 64.7 Ethanol: 0.78 78.4 1.22 –114.6 –1.99 K b [2] Ethylene bromide: 2.18 133 6.43 9.974 –12.5 K b & K f [1] Ethylene glycol: 1.11 197.3 2.26 −12.9 ...
Carnoy's solution is a fixative composed of 60% ethanol, 30% chloroform and 10% glacial acetic acid, 1 gram of ferric chloride. [1] [2]Carnoy's solution is also the name of a different fixation composed of ethanol and glacial acetic acid (3:1).
Chloroform could also be mixed with other anaesthetic agents such as ether to make C.E. mixture, or ether and alcohol to make A.C.E. mixture. [citation needed] In 1848, Hannah Greener, a 15-year-old girl who was having an infected toenail removed, died after being given the anaesthetic. [57]
Chloroform: Chloroform is stabilized with small quantities of amylene or ethanol, because exposure of pure chloroform to oxygen and ultraviolet light produces phosgene gas. Some chloroform solutions come as pre-made a 96% chloroform, 4% isoamyl alcohol mixture that can be mixed with an equal volume of phenol to obtain the 25:24:1 solution.
Ethanol can also be used as a feedstock. This reaction is catalyzed by antimony trichloride: H 3 CCHO + 3 Cl 2 + H 2 O → Cl 3 CCH(OH) 2 + 3 HCl. The chloral hydrate is distilled from the reaction mixture. The distillate is then dehydrated with concentrated sulfuric acid, after which the heavier acid layer (containing the water) is drawn off:
108.52 g·mol −1 Appearance ... Preparation. Ethyl chloroformate can be prepared using ethanol and phosgene: Safety Ethyl chloroformate is a highly toxic, flammable ...