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A McCabe–Thiele diagram for the distillation of a binary (two-component) feed is constructed using the vapor-liquid equilibrium (VLE) data—which is how vapor is concentrated when in contact with its liquid form—for the component with the lower boiling point. Figure 1: Typical McCabe–Thiele diagram for distillation of a binary feed
Distillation Design is a book which provides complete coverage of the design of industrial distillation columns for the petroleum refining, chemical and petrochemical plants, natural gas processing, pharmaceutical, food and alcohol distilling industries.
In this case the mixture components A and B are separated in the first column through the solvent E (recovered in the second column). Extractive distillation is defined as distillation in the presence of a miscible , high-boiling, relatively non-volatile component, the solvent , that forms no azeotrope with the other components in the mixture.
An overhead condenser is a heat exchange equipment used for condensing the mixture leaving the top of the column. Either cooling water or air is used as a cooling agent. An overhead accumulator is a horizontal pressure vessel containing the condensed mixture. Pumps can be used to control the reflux to the column.
Fractionation at total reflux. The Fenske equation in continuous fractional distillation is an equation used for calculating the minimum number of theoretical plates required for the separation of a binary feed stream by a fractionation column that is being operated at total reflux (i.e., which means that no overhead product distillate is being withdrawn from the column).
Chemical engineering schematic of typical bubble-cap trays in a distillation tower. Design and operation of a distillation column depends on the feed and desired products. Given a simple, binary component feed, analytical methods such as the McCabe–Thiele method [4] [6] [7] or the Fenske equation [4] can be used.
Schematics of a plate column with bubble cap trays. The feed to the column can be liquid, gas or gas and liquid at equilibrium. Inside the column there are always two phases: one gas phase and one liquid phase. The liquid phase flows downward through the column via gravity, [1] while the gas phase flows upward.
The apparatus shown in the diagram represents a batch distillation as opposed to a continuous distillation. The liquid feed mixture to be distilled is placed into the round-bottomed flask along with a few anti-bumping granules, and the fractionating column is fitted into the top. As the mixture is heated and boils, vapor rises up the column.