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The Buchner ring expansion is a two-step organic C-C bond forming reaction used to access 7-membered rings. The first step involves formation of a carbene from ethyl diazoacetate , which cyclopropanates an aromatic ring.
Buchner funnels are made of porcelain and include a plate of sintered glass or perforated porcelain. These are used in filtration under low pressure with a Buchner flask. [2] Hot filtration funnel is a less commonly seen funnel where the funnel is jacketed, and surrounded by a heated fluid. [3]
A Büchner funnel is a piece of laboratory equipment used in filtration. [1] It is traditionally made of porcelain , but glass and plastic funnels are also available. On top of the funnel-shaped part there is a cylinder with a fritted glass disc/perforated plate separating it from the funnel.
A Büchner flask, also known as a vacuum flask, [1] filter flask, suction flask, side-arm flask, or Bunsen flask, is a thick-walled Erlenmeyer flask with a short glass tube and hose barb protruding about an inch from its neck.
A separatory funnel, also known as a separation funnel, separating funnel, or colloquially sep funnel, is a piece of laboratory glassware used in liquid-liquid extractions to separate (partition) the components of a mixture into two immiscible solvent phases of different densities. [1]
Ernst Wilhelm Büchner (18 March 1850 – 25 April 1924) was the German industrial chemist after whom the Büchner flask and Büchner funnel are named. The patent for his two inventions was published in 1888.
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Initial steps in the Buchner–Curtius–Schlotterbeck reaction mechanism. The reaction is then completed either by the reformation of the carbonyl through an 1,2-rearrangement or by the formation of the epoxide. There are two possible carbonyl products: one formed by migration of R 1 (4) and the other by migration of R 2 (5). The relative ...