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The dish is then closed and heated at high temperature until completely clean, fused silica is produced. Comparison of the initial weight of the substance and that of the fused silica allows the content of silicon in the sample to be determined. A generic evaporator dish. The shape of the evaporating dish encourages evaporation in two ways:
The experiment uses a simple barometer to measure the pressure of air, filling it with mercury up until 75% of the tube. Any air bubbles in the tube must be removed by inverting several times. After that, a clean mercury is filled once again until the tube is completely full. The barometer is then placed inverted on the dish full of mercury.
In laboratory and other scientific settings, they are usually referred to simply as flasks. Flasks come in a number of shapes and a wide range of sizes, but a common distinguishing aspect in their shapes is a wider vessel "body" and one (or sometimes more) narrower tubular sections at the top called necks which have an opening at the top.
This is needed for the oven due to its high temperatures that can reach up to 500 degrees Celsius. Other forms of the laboratory oven include vacuum ovens, forced air convection ovens, and gravity convection ovens. [1] Forensic labs use vacuum ovens that have been configured in specific ways to assist in developing fingerprints.
A rotary evaporator [1] (rotovap) is a device used in chemical laboratories for the efficient and gentle removal of solvents from samples by evaporation.When referenced in the chemistry research literature, description of the use of this technique and equipment may include the phrase "rotary evaporator", though use is often rather signaled by other language (e.g., "the sample was evaporated ...
The main feature of thermodynamic diagrams is the equivalence between the area in the diagram and energy. When air changes pressure and temperature during a process and prescribes a closed curve within the diagram the area enclosed by this curve is proportional to the energy which has been gained or released by the air.
Diagram of a vacuum flask Gustav Robert Paalen, Double Walled Vessel. Patent 27 June 1908, published 13 July 1909 Patent 27 June 1908, published 13 July 1909 The vacuum flask was designed and invented by Scottish scientist James Dewar in 1892 as a result of his research in the field of cryogenics and is sometimes called a Dewar flask in his honour.
Then the partial pressure of its vapor must be considered when obtaining its condensation temperature. For example, if the gas entering the condenser is a mixture of 25% ethanol vapor and 75% carbon dioxide (by moles) at 100 kPa (typical atmospheric pressure), the condensation surface must be kept below 48 °C, the boiling point of ethanol at ...