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Zinc smelting has historically been more difficult than the smelting of other metals, e.g. iron, because in contrast, zinc has a low boiling point. At temperatures typically used for smelting metals, zinc is a gas that will escape from a furnace with the flue gas and be lost, unless specific measures are taken to prevent it.
The Tipson–Cohen reaction is a name reaction first discovered by Stuart Tipson and Alex Cohen at the National Bureau of Standards in Washington D.C. [1] The Tipson–Cohen reaction occurs when two neighboring secondary sulfonyloxy groups in a sugar molecule are treated with zinc dust (Zn) and sodium iodide (NaI) in a refluxing solvent such as N,N-dimethylformamide (DMF) to give an ...
Uranyl zinc acetate (ZnUO 2 (CH 3 COO) 4) is a compound of uranium.. Uranyl zinc acetate is used as a laboratory reagent in the determination of sodium concentrations of solutions using a method of quantitatively precipitating sodium with uranyl zinc acetate and gravimetrically determining the sodium as uranyl zinc sodium acetate, (UO 2) 3 ZnNa(CH 3 CO 2) 9 ·6H 2 O.
This is a list of analysis methods used in materials science. Analysis methods are listed by their acronym, if one exists. Analysis methods are listed by their acronym, if one exists. Contents:
The Knorr pyrrole synthesis is a widely used chemical reaction that synthesizes substituted pyrroles (3). [1] [2] [3] The method involves the reaction of an α-amino-ketone (1) and a compound containing an electron-withdrawing group (e.g. an ester as shown) α to a carbonyl group (2). [4] The Knorr pyrrole synthesis
The procedure uses different solvents and flames to view the test flame through a cobalt blue glass or didymium glass to filter the interfering light of contaminants such as sodium. [12] Flame tests are subject of a number of limitations. The range of elements positively detectable under standard conditions is small.
The Merrill–Crowe Process is a separation technique for removing gold from the solution obtained by the cyanide leaching of gold ores. It is an improvement of the MacArthur-Forrest process, where an additional vacuum is managed to remove air in the solution (invention of Crowe), and zinc dust is used instead of zinc shavings (improvement of Merrill).
The Simmons–Smith reagent is used to prepare cyclopropanes from olefin using methylene iodide as the methylene source. The reaction is effected with zinc. The key zinc-intermediate formed is a carbenoid (iodomethyl)zinc iodide which reacts with alkenes to afford the cyclopropanated product. The rate of forming the active zinc species is ...