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The McCabe–Thiele method is a technique that is commonly employed in the field of chemical engineering to model the separation of two substances by a distillation column. [ 1 ] [ 2 ] [ 3 ] It uses the fact that the composition at each theoretical tray is completely determined by the mole fraction of one of the two components.
Distillation Design is a book which provides complete coverage of the design of industrial distillation columns for the petroleum refining, chemical and petrochemical plants, natural gas processing, pharmaceutical, food and alcohol distilling industries.
Chemical engineering schematic of typical bubble-cap trays in a distillation tower. Design and operation of a distillation column depends on the feed and desired products. Given a simple, binary component feed, analytical methods such as the McCabe–Thiele method [4] [6] [7] or the Fenske equation [4] can be used.
Modeling and simulation of batch distillation unit is done with the help of one of the most important process simulators (aspen plus) used in chemical industry with the following data given in the table and check the simulation result. Various steps are involved in the simulation of batch distillation column using aspen plus software is :
The heat entering a distillation column is a crucial operating parameter, addition of excess or insufficient heat to the column can lead to foaming, weeping, entrainment, or flooding. Figure 3 depicts an industrial fractionating column separating a feed stream into one distillate fraction and one bottoms fraction.
The pressure at the top is maintained at 1.2–1.5 atm [2] so that the distillation can be carried out at close to atmospheric pressure, and therefore it is known as the atmospheric distillation column. [3] The vapors from the top of the column are a mixture of hydrocarbon gases and naphtha, at a temperature of 120 °C–130 °C.
The calculation process requires the availability of a great deal of vapor–liquid equilibrium data for the components present in the distillation feed, and the calculation procedure is very complex. [2] [3] In an industrial distillation column, the N t required to achieve a given separation also depends upon the amount of reflux used. Using ...
Fractionation at total reflux. The Fenske equation in continuous fractional distillation is an equation used for calculating the minimum number of theoretical plates required for the separation of a binary feed stream by a fractionation column that is being operated at total reflux (i.e., which means that no overhead product distillate is being withdrawn from the column).