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A cooling bath or ice bath, in laboratory chemistry practice, is a liquid mixture which is used to maintain low temperatures, typically between 13 °C and −196 °C. These low temperatures are used to collect liquids after distillation , to remove solvents using a rotary evaporator , or to perform a chemical reaction below room temperature ...
Vitrification is a flash-freezing (ultra-rapid cooling) process that helps to prevent the formation of ice crystals and helps prevent cryopreservation damage. Researchers Greg Fahy and William F. Rall helped to introduce vitrification to reproductive cryopreservation in the mid-1980s. [ 23 ]
Defrosting a freezer with an improvised water collection method. In refrigerators, defrosting (or thawing) is the removal of frost and ice.. A defrosting procedure is generally performed periodically on refrigerators and freezers to maintain their operating efficiency.
Freeze drying, also known as lyophilization or cryodesiccation, is a low temperature dehydration process [1] that involves freezing the product and lowering pressure, thereby removing the ice by sublimation. [2] This is in contrast to dehydration by most conventional methods that evaporate water using heat. [3]
A cold finger is a piece of laboratory equipment that is used to generate a localized cold surface. It is named for its resemblance to a finger and is a type of cold trap . The device usually consists of a chamber that a coolant fluid (cold tap water, or perhaps something colder) can enter and leave.
In practice, a mechanical freezing process is usually used instead due to cost. There has been continuous optimization of the freezing rate in mechanical freezing to minimize ice crystal size. [2] Flash freezing techniques are also used to freeze biological samples quickly so that large ice crystals cannot form and damage the sample. [5]
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In this laboratory-scale technique, the fluid to be degassed is placed in a Schlenk flask and flash-frozen, usually with liquid nitrogen. Next a vacuum is applied, perhaps to attain a vacuum of 1 mm Hg (for illustrative purposes). The flask is sealed from the vacuum source, and the frozen solvent is allowed to thaw. Often, bubbles appears upon ...