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A Soxhlet extractor is a piece of laboratory apparatus [1] invented in 1879 by Franz von Soxhlet. [2] It was originally designed for the extraction of a lipid from a solid material. Typically, Soxhlet extraction is used when the desired compound has a limited solubility in a solvent , and the impurity is insoluble in that solvent.
Extraction in chemistry is a separation process consisting of the separation of a substance from a matrix. The distribution of a solute between two phases is an equilibrium condition described by partition theory.
The extraction cell is filled with the solid sample to be examined and placed in a temperature-controllable oven. After adding the solvent, the cell is heated at constant pressure (adjustable between 0.3 and 20 MPa) up to a maximum temperature of 200°C and kept at constant conditions for a while so that equilibrium can be established.
Supercritical Fluid Extraction - Principles and Practice. Butterworth Heinemann series in chemical engineering (2nd ed.). Butterworth Heinemann. ISBN 978-0-7506-9244-1. Taylor, Larry T (1996). Supercritical Fluid Extraction. Techniques in analytical chemistry. John Wiley and Sons, Inc. ISBN 978-0-471-11990-6
2: Still pot (extraction pot) - still pot should not be overfilled and the volume of solvent in the still pot should be 3 to 4 times the volume of the soxhlet chamber. 3: Distillation path 4: Soxhlet Thimble
Solid-phase extraction (SPE) [1] is a solid-liquid extractive technique, by which compounds that are dissolved or suspended in a liquid mixture are separated, isolated or purified, from other compounds in this mixture, according to their physical and chemical properties. Analytical laboratories use solid phase extraction to concentrate and ...
Exhaustive Soxhlet extraction after polymerization with polar solvents was found to effectively fractionate the polymer and remove residual catalyst before NMR spectroscopy. [30] Using a lower ratio of catalyst to monomer (2:1, rather than 4:1) may increase the regioregularity of poly(3-dodecylthiophene)s. [58]
Soxhlet extraction This has been a standard extraction method with organic solvents since its creation over a century ago. This technique consists of placing the MIP particles into a cartridge inside the extraction chamber, and the extraction solvent in poured into a flask connected to the extractor chamber.